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SOP for Calibration of Micro Controller Melting Point Apparatus

OBJECTIVE
To provide a procedure for the calibration of the microcontroller melting point apparatus.

SCOPE
Applicable to the microcontroller melting point apparatus in QC Chemistry.

RESPONSIBILITY
  • The task shall be performed by QC Executive.
  • It is the responsibility of the Manager QC to ensure that this procedure is followed accordingly.

PROCEDURE
  • Set up the instrument as per the standard operating procedure.
  • Use the following reference standards to calibrate the instrument, and record the observation in Attachment-I.
  1. Vanillin
  2. Acetanilide
  3. Sulphanilamide
  4. Caffeine


  • The melting point of the reference standards should be within the standard range
  • The standard melting point range shall be taken from the COA of the standard.
  • Calibration should be carried out once every six months or after maintenance of the instrument.


ATTACHMENT
Attachment 1: Calibration record of Micro Controller Melting Point Apparatus

ABBREVIATION
QC- Quality Control
COA - Certificate of Analysis

REVISION HISTORY
Nil

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